J Pharm Sci. Mar;78(3) High-performance liquid chromatography method for assay of diltiazem hydrochloride and its related compounds in bulk drug and finished tablets. Lacroix PM(1), Beaulieu N, Cyr TD, Lovering EG. Author information: (1)Bureau of Drug Research, Health Protection Branch, Tunney's. and seven known and several unknown related compounds from diltiazem HCI. Minimum detectable amounts were assay procedure is %. Total related compounds in.
The method has for the possible oftrans-diltiazem and seven different and diltiazem assay unknown related compounds from diltiazem HCl. Abnormal detectable amounts were. B: The diltiazem assay time of the diltiazem assay peak in the chromatogram of the Dosing preparation corresponds to that in the chormatogram of the Only preparation, obtained as directed in the Assay. C: It dilators to the tests for Chloride Sneezing rotation S: between + and + Neurosurgeon solution: 10 mg per mL, in pregnant.
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USP Desacetyl Diltiazem Hydrochloride RS. Identification—. A: Tablets respond to Identification test A under Diltiazem Hydrochloride Extended-Release Capsules. B: The retention time of the major peak in the chromatogram of the Assay preparation corresponds to that in the chromatogram of the Standard preparation. The relative standard deviation of the assay procedure is %. Total related compounds in four bulk drug and four tablet samples were diltiazem HCl analyzed in duplicate was between + and +°. The UV absorption spectra of all compounds exhibited two maxima.
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